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纯钽TIG接头的组织和性能研究

Study on microstructure and properties of pure tantalum TIG joint

  • 摘要: 对纯钽TIG接头开展组织、力学性能及热处理工艺研究. 采用工业计算机断层扫描(computed tomography, CT)、OM和SEM表征接头微观组织,利用显微硬度计及万能试验机测试接头显微硬度、拉伸性能和弯曲性能. 结果表明, 焊接参数对焊缝成形起决定性作用,焊接电流过小导致未焊透,焊接电流过大导致烧穿. 焊接速度过大产生未焊透及咬边,焊接速度过小导致热影响区宽度增大. 优选出焊接电流为280 ~ 320 A、焊接速度为150 ~ 180 mm/min为工艺窗口,该参数下接头抗拉强度最高达262 MPa,断口呈韧窝特征,断裂均起始于热影响区,并沿靠近熔合区的软化区域扩展. 在优选参数基础上研究热处理温度影响,发现随退火温度升高,焊缝残余应力由142.17 MPa显著降至退火温度为1320 ℃的10.69 MPa,抗拉强度因晶粒粗化降至194 MPa. 综合应力消除效果与性能损失,确定优选退火温度为1320 ℃. 应用优选工艺焊接实际结构,经无损检测与金相验证,接头内部无缺陷,质量良好.

     

    Abstract: Conduct research on the microstructure, mechanical properties, and heat treatment process of pure tantalum TIG joints. Industrial computed tomography (CT), OM, and SEM were used to characterize the microstructure of the joint, and microhardness tester and universal testing machine were used to test the hardness, tensile, and bending properties of the joint. The results indicate that welding parameters play a decisive role in the formation of the weld seam. Low current leads to incomplete penetration, while high current leads to burn through; Excessive speed results in incomplete penetration and undercutting, while excessive speed widens the heat affected zone. Selecting a welding current of 280 ~ 320 A and a speed of 150 ~ 180 mm/min as the process window, the maximum tensile strength of the joint under these parameters is 262 MPa, and the fracture surface exhibits ductile dimples. The fracture starts from the heat affected zone and extends along the softened zone near the fusion zone. On the basis of optimizing parameters, the influence of heat treatment temperature was studied, and it was found that with the increase of annealing temperature, the residual stress of the weld seam significantly decreased from 142.17 MPa to 10.69 MPa (1320 ℃), and the tensile strength decreased to 194 MPa due to grain coarsening. Based on the comprehensive stress relief effect and performance loss, 1320 ℃ is determined as the optimal heat treatment temperature. The actual structural components were welded using the preferred welding process, and after non-destructive testing and metallographic verification, there were no defects inside the joint, indicating good quality.

     

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