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等离子弧增材制造AlCoCrFeNi2.1共晶高熵合金工艺及组织和性能

Plasma arc additive manufacturing of AlCoCrFeNi2.1 high-entropy alloy process and organizational properties research

  • 摘要: 采用等离子弧增材制造技术,通过单一控制变量法研究了不同工艺参数对AlCoCrFeNi2.1共晶高熵合金组织和性能的影响,得到增材件优化参数,研究不同热循环次数对增材薄壁件组织和性能的影响. 结果表明,当熔敷电流为130 A、熔敷速度5 mm/s、送粉转速2 r/min时,获得表面无明显缺陷、高成形系数和高硬度的沉积层;随着沉积层逐层叠加,底部区域热循环层数最多,使BCC相溶解到FCC相中,组织晶粒粗化,导致底部硬度最低,而顶部较高,增材件平均硬度为339.70 HV0.5 ± 4.89 HV0.5;随着软质相FCC相自下而上晶粒变小且含量降低,使抗拉强度和塑性逐渐降低,而屈服强度略有提高,纵向试样的力学性能要优于横向试样,表现出明显各向异性,抗拉强度可高达1131.17 MPa ± 34.39 MPa、屈服强度为594.66 MPa ± 3.71 MPa、断后伸长率为16.47% ± 2.21%.

     

    Abstract: Using plasma arc additive manufacturing technology, the influence of different process parameters on the organization and properties of AlCoCrFeNi2.1 eutectic high entropy alloy was studied by single control variable method, to obtain the optimization parameters of the additives, and to study the influence of different number of thermal cycles on the organization and properties of the additive thin-walled. The results show that when the melting current is 130 A, the melting speed is 5 mm/s, and the powder feeding rotational speed is 2 r/min, the deposited layer with no obvious surface defects, high molding coefficient and high hardness is obtained. As the deposited layers are stacked layer by layer, the bottom region has the highest number of thermocycling layers, which dissolves the BCC phase into the FCC phase and coarsens the tissue grain, resulting in the lowest hardness at the bottom and higher at the top. The average hardness of the additive is 326.64 HV0.5 ± 2.04 HV0.5. With the soft phase, the FCC phase, the grains become smaller and the content of FCC phase decreases from the bottom to the top, which leads to the gradual decrease in tensile strength and plasticity and a slight increase in yield strength. The mechanical properties of the longitudinal specimens are better than those of the transverse specimens, showing obvious anisotropy, and the tensile strength can be as high as 1131.17 MPa ± 34.39 MPa, the yield strength of 594.66 MPa ± 3.71 MPa, and the elongation at break of 16.47% ± 2.21%.

     

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