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IC10单晶过渡液相扩散焊接头微观组织与力学性能

Microstructure and mechanical properties of IC10 single crystal superalloy transient liquid phase diffusion bonding joint

  • 摘要: 采用扫描电镜(SEM)和能谱分析仪(EDS)研究IC10单晶高温合金过渡液相(TLP)扩散焊接头微观组织演变.结果表明,接头由连接区和基体区所组成,连接区由等温凝固区和快速凝固区组成.快速凝固区可以通过延长保温时间的方法予以消除.随着保温时间从2 h增加到8 h,基体内的γ'相尺寸达到了0.9μm.通过限制TLP扩散焊接头内晶界的形成,以及焊后固溶处理的方法可以有效提高接头的力学性能.在温度1 000℃下,接头平均抗拉强度为507 MPa.在温度1 000℃、应力144 MPa下接头持久寿命可达到120 h以上.

     

    Abstract: Microstructural evolution of transient liquid phase(TLP) diffusion bonding joint of IC10 single crystal superalloy was investigated with scanning electron microscopy(SEM) and energy-dispersive spectrum(EDS).The results show that the joint contained bonding zone and base material zone.The bonding zone consisted of isothermal solidification zone and rapid solidification zone.Rapid solidification zone could be eliminated by increasing welding time.The size of γ' phase in the base material reached 0.9 μm when the welding time increased from 2 h to 8 h.The mechanical properties of the joints can be effectively improved by restraining formation of grain boundary in TLP diffusion bonding joint and postweld solution treatment.The average tensile strength of the joints was 507 MPa at 1 000℃.The creep rupture life of the joints reached 120 h under the condition of 144 MPa stress at 1 000℃.

     

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