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纳米粉末对轴向等离子喷涂TiB2-Al2O3复合涂层的影响

Effects of nanoscale powder on coating deposited by axial plasma spraying TiB2/Al2O3 composite powders

  • 摘要: 采用三阴极轴向送粉等离子喷涂制备TiB2/Al2O3陶瓷复合涂层,其中一种喷涂粉末是自蔓延高温合成的常规微米级TiB2/Al2O3复合粉末,另一种是由TiB2/Al2O3复合粉掺杂质量分数10%的纳米Al2O3粉经喷雾干燥造粒制备的纳微米结构喂料。比较研究两种涂层的微观组织、耐磨性能,探讨纳米粉末对涂层的影响:扫描电镜、X射线衍射分析涂层微观结构和物相组成;转盘磨损试验测试涂层的耐磨性能。结果显示两种涂层表面洛氏硬度相当,纳米掺杂涂层组织致密性、耐磨性明显高于常规粉末涂层,以及TiB2的氧化产物TiO2含量低于常规粉末涂层。

     

    Abstract: TiO2/Al2O3 composite coatings were deposited by axial plasma spraying (Mettch Axial-Ⅲ):one of feedstock powders was conventional micrometer powder derived from self-propagating high temperature synthesis process, and the other was fabricated by spray-drying TiO2/Al2O3 composite powder doped with 10% mass fraction nanosize Al2O3 powder.Microstructure and wear resistance of two type coatings were compared, and effects of nanoscale powder on the coatings were investigated.Scanning electron microscope and X-ray diffraction analysis were used to analyze the sprayed coatings, and disc abrasive wear apparatus was employed to test wear resistance of the coatings. Results show that density and wear resistance of sprayed coating from spray-drying powder are better than that from conventional powder, TiO2 content is also less than that in the coating from conventional powder, and superficial Rockwell Hardnesses of two coatings are about the same.

     

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