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涂层梯度液相烧结的原理和显微组织

The Principle and Micro-structure of Gradient Liquid Phase Sintering of Thermal Spray Coating

  • 摘要: 讨论了均匀粉末压坯烧结时因热传导而产生的温度分布存在时间和空间上的异步现象,阐明了涂层烧结时梯度设计的必要性。分析了喷涂层梯度液相烧结的基本条件,并观察了其显微组织及其结合性能。结果表明,采用梯度设计可实现涂层稳定成形所需的液相烧结,避免了常规液相烧结时涂层的粘弹性流动。显微组织中氧化物有球化趋势,表层存在明显固-液相分界线,基材界面出现了冶金结合。

     

    Abstract: In this paper, the non-synchronous phenomenon of temperature distribution in space and time in compact metal-power sintering are discussed, it indicate that the gradient design for thermal spray coating sintering is necessary. The basic condition of gradient liquid phase sintering, the microstructure and the poperty of coating bonding are discussed.The results show that the liquid phase sintering necessary for coating stability can be realized by gradient designing, the viscous flow of ordinary liquid phase sintering can be avoided, the oxide in micro-structure tend to assembling, and there is a clear liquid-solid phase boundary line in the surface of coating.

     

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