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CNTs-GNPs/K418复合材料SLM工艺优化

SLM process optimization of CNTs-GNPs/K418 composites

  • 摘要: 为了满足航空航天发动机热端部件对镍基高温合金日益提升的使用性能要求,采用选区激光熔化(selective laser melting,SLM)技术制备碳纳米管-石墨烯纳米片(carbon nanotubes - graphene nanosheets,CNTs-GNPs)/K418复合材料,通过L9(34)正交试验研究激光功率、扫描速度、扫描间距及铺粉层厚对其成形质量与力学性能的影响,基于能量密度揭示工艺参数与打印件组织性能的关联机制.结果表明,在文中的工艺参数下,激光功率、扫描间距越大,扫描速度、铺粉层厚越小,抗拉强度越高;激光功率对平均抗拉强度影响最显著,影响顺序为激光功率、铺粉层厚、扫描速度和扫描间距.能量密度过高(141.7 J/mm3)且扫描间距较小时,会因Marangoni对流加剧以及热应力集中产生气孔与裂纹;能量密度过低(≤37.9 J/mm3)会导致未熔合与孔隙增多.当能量密度为95.8 J/mm3时,试样无明显缺陷,横截面形成连续蜂窝状胞晶,纵截面呈典型柱状晶定向生长,抗拉强度可达到934.5 MPa.文中研究成果可为高性能高温部件增材制造技术提供工艺支撑.

     

    Abstract: In order to meet the increasingly high performance requirements of nickel-based superalloys for the hot-end components of aerospace engines, carbon nanotubes-graphene nanosheets(CNTs-GNPs)/K418 composites were prepared using selective laser melting (SLM) technology. Through the L9 (34) orthogonal experiment, the effects of laser power, scanning speed, scanning interval, and powder layer thickness on the forming quality and mechanical properties were studied. Based on the energy density, the correlation mechanism between process parameters and the structure and properties of the printed parts was revealed. The results show that under the process parameters in the paper, the larger the laser power and scan spacing, and the smaller the scan speed and powder layer thickness, the higher the tensile strength; laser power has the most significant effect on the average tensile strength, with the order of influence being: laser power > powder layer thickness > scan speed > scan spacing. Excessively high energy density (141.7 J/mm3) combined with small scanning spacing can lead to pores and cracks due to intensified Marangoni convection and concentrated thermal stress. Excessively low energy density (≤37.9 J/mm3) results in lack of fusion and increased porosity. When energy density is 95.8 J/mm3, there are no obvious defects in the sample; the cross-section forms a continuous honeycomb-like cell structure, and the longitudinal section shows typical columnar crystal-oriented growth, with tensile strength reaching 934.5 MPa. The research results in the paper can provide process support for the additive manufacturing technology of high-performance high-temperature components.

     

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